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polymer content is fixed at 2% and the amount of clay is varied, as well as the 2% polymer-3% clay solutions of pri-mary interest in our previousstudy [14]. The combinationof SANS, light scattering, optical microscopy and rheometry provides a more complete physical picture of the shear re-sponse of these intriguingsuspensions,which in turn.
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polymer. Through a combination of SANS and rheology, shear gelation is found to occur through the deformation of large stable flocs that expose fresh surface area for the formation of new polymer bridges. At rest, the temporary shear-induced flocs slowly fractionate with time as the polymer desorbs from the clay surface.
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Small-angle neutron scattering (SANS) is a powerful technique that has been widely used to study polymer materials. In particular, it can provide information on the size, shape, and structure of polymers as well as associated thermodynamic quantities.
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The shear orientation of viscoelastic clay-polymer solutions was investigated by means of rheology, flow birefringence and small-angle neutron scattering (SANS)
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Unusual Rheological Behavior of Liquid Polybutadiene Rubber/Clay Nanocomposite Gels: The Role of Polymer−Clay Interaction, Clay Exfoliation, and Clay Orientation and Disorientation. Macromolecules 2006 , 39 (19) , 6653-6660.
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With increasing shear rate, clay particles oriented first (SANS on regular samples) and then polymer chains started to stretch (SANS on contrast matched samples). Cessation of shear led to fast recovery, demonstrating the system to be highly elastic. Introduction
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Clay Abstract The influence of shear on viscoelastic polymer−clay solutions was investigated by means of small-angle neutron scattering (SANS) under shear. SANS was used to measure the shear-induced orientation of polymer and platelets. With increasing shear rate an anisotropic scattering pattern developed.
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Through the demonstration of applications in sample systems such as polymer solutions, polymer blend, semi-crystalline polymer, polymer nano-composites, hydrogel, and bio-materials, the advantages of SANS on soft-matters are demonstrated.
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Created December 31, 2001, Updated October 12, 2021 The influence of shear on viscoelastic polymer-clay solutions was investigated by means of small-angle neutron scattering (SANS) under shear.
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The colloidal and rheological properties of poly-mer-clay nanocomposites gels and solutions1 have received considerable attention in the liter-ature, and good reviews are available.2-4 Platelet ordering at the nanometer length scale is a chal-lenging and active area of research in materials science.
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Recent developments in small-angle neutron scattering (SANS) investigations on polymer gels are reviewed by encompassing (i) volume phase transition and microphase separation, (ii).
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SANS study unpicks this phenomenon to find that gelation occurs with concurrent aggregation of BCS in the bulk, inducing clay-clay interactions only in lower Mn BCS systems with large nanoaggregates.. and as such the development of polymer/clay hybrid materials which can add function to the native clay behaviour are of great interest. BCS.
